真空辅助挥发-便携式气相色谱-质谱现场快速测定锂电池微漏

陆欣鑫; 张硕; 徐恺; 仇俊炜; 朱惠君; 陈雨琳; 李晓旭

doi:10.7538/zpxb.2024.0126

[1]

LI M, LU J, CHEN Z, AMINE K. 30 years of lithium-ion batteries[J]. Advanced Materials, 2018, 30(33): 1 800 561.

[2]

KWADE A, HASELRIEDER W, LEITHOFF R, MODLINGER A, DIETRICH F, DROEDER K. Current status and challenges for automotive battery production technologies[J]. Nature Energy, 2018, 3(4): 290 - 300 . doi: 10.1038/s41560-018-0130-3

[3]

AISSOU S, REKIOUA D, MEZZAI N, REKIOUA T, BACHA S. Modeling and control of hybrid photovoltaic wind power system with battery storage[J]. Energy Conversion and Management, 2015, 89: 615 - 625 . doi: 10.1016/j.enconman.2014.10.034

[4]

GAO T, WANG Z, CHEN S, GUO L. Hazardous characteristics of charge and discharge of lithium-ion batteries under adiabatic environment and hot environment[J]. International Journal of Heat and Mass Transfer, 2019, 141: 419 - 431 . doi: 10.1016/j.ijheatmasstransfer.2019.06.075

[5]

WANG Z, OUYANG D, CHEN M, WANG X, ZHANG Z, WANG J. Fire behavior of lithium-ion battery with different states of charge induced by high incident heat fluxes[J]. Journal of Thermal Analysis and Calorimetry, 2018, 136(6): 2 239-2 247.

[6]

DU X, YANG B, LU Y, GUO X, ZU G, HUANG J. Detection of electrolyte leakage from lithium-ion batteries using a miniaturized sensor based on functionalized double-walled carbon nanotubes[J]. Journal of Materials Chemistry C, 2021, 9(21): 6 760-6 765.

[7]

LIU C, WAN J, DONG W, WANG X, CHEN J, LI S, MAO C, ZENG D. Rapid detection of ppb level electrolyte leakage of lithium ion battery (LIB) by WO₃ hollow microsphere gas sensor[J]. Materials Today Communications, 2023, 35: 106 398.

[8]

LU Y, ZHANG S, DAI S, LIU D, WANG X, TANG W, GUO X, DUAN J, LUO W, YANG B, ZOU J, HUANG Y, KATZ H E, HUANG J. Ultrasensitive detection of electrolyte leakage from lithium-ion batteries by ionically conductive metal-organic frameworks[J]. Matter, 2020, 3(3): 904 - 919 . doi: 10.1016/j.matt.2020.05.021

[9]

WANG H, XIONG R, CUI Z, WAN J, SA B, WU X, SONG W, WANG X, ZENG D. Ultrasensitive detection for lithium-ion battery electrolyte leakage by rare-earth Nd-doped SnO₂ nanofibers[J]. ACS Sensors, 2023, 8(4): 1 700-1 709.

[10]

ESSL C, SEIFERT L, RABE M, FUCHS A. Early detection of failing automotive batteries using gas sensors[J]. Batteries, 2021, 7(2): 25 . doi: 10.3390/batteries7020025

[11]

MATEEV V, MARINOVA I, KARTUNOV Z. Gas leakage source detection for Li-ion batteries by distributed sensor array[J]. Sensors, 2019, 19(13): 2 900.

[12]

ZHANG E, YAN W, ZHOU S, LING M, ZHOU H. Fe₃O₄@uio66 core-shell composite for detection of electrolyte leakage from lithium-ion batteries[J]. Nanotechnology, 2023, 34(13): 135 501.

[13]

HORSTHEMKE F, FRIESEN A, MÖNNIGHOFF X, STENZEL Y P, GRÜTZKE M, ANDERSSON J T, WINTER M, NOWAK S. Fast screening method to characterize lithium ion battery electrolytes by means of solid phase microextraction-gas chromatography-mass spectrometry[J]. RSC Advances, 2017, 7(74): 46 989-46 998.

[14]

SUN J, LI J, ZHOU T, YANG K, WEI S, TANG N, DANG N, LI H, QIU X, CHEN L. Toxicity, a serious concern of thermal runaway from commercial Li-ion battery[J]. Nano Energy, 2016, 27: 313 - 319 . doi: 10.1016/j.nanoen.2016.06.031

[15]

YU S, XIONG J, WU D, LYU X, YAO Z, XU S, TANG J. Pyrolysis characteristics of cathode from spent lithium-ion batteries using advanced TG-FTIR-GC/MS analysis[J]. Environmental Science and Pollution Research, 2020, 27(32): 40 205-40 209.

[16]

MöNNIGHOFF X, MURMANN P, WEBER W, WINTER M, NOWAK S. Post-mortem investigations of fluorinated flame retardants for lithium ion battery electrolytes by gas chromatography with chemical ionization[J]. Electrochimica Acta, 2017, 246: 1 042-1 051.

[17]

HENSCHEL J, WIEMERS-MEYER S, DIEHL M, LURENBAUM C, JIANG W, WINTER M, NOWAK S. Preparative hydrophilic interaction liquid chromatography of acidic organofluorophosphates formed in lithium ion battery electrolytes[J]. Journal of Chromatography A, 2019, 1 603: 438-441.

[18]

SAVIGNAC L, DAWKINS J I G, SCHOUGAARD S B, MAUZEROLL J. Determining the effect of dissolved CO₂ on solution phase Li⁺ diffusion in common Li-ion battery electrolytes[J]. Electrochemistry Communications, 2021, 125: 106 979.

[19]

DOHMANN J F, HORSTHEMKE F, KÜPERS V, BLOCH S, PREIBISCH Y, KOLESNIKOV A, KOLEK M, STAN M C, WINTER M, BIEKER P. Galvanic couples in ionic liquid-based electrolyte systems for lithium metal batteries-an overlooked cause of galvanic corrosion?[J]. Advanced Energy Materials, 2021, 11(24): 2 101 021.

[20]

PARHIZI M, CACERES-MARTINEZ L E, MODEREGER B A, KENTTÄMAA H I, KILAZ G, OSTANEK J K. Determining the composition of carbonate solvent systems used in lithium-ion batteries without salt removal[J]. Energies, 2022, 15(8): 2 805.

[21]

HENSCHEL J, PESCHEL C, GÜNTER F, REINHART G, WINTER M, NOWAK S. Reaction product analysis of the most active “inactive” material in lithium-ion batteries-the electrolyte. II: battery operation and additive impact[J]. Chemistry of Materials, 2019, 31(24): 9 977-9 983.

[22]

HORSTHEMKE F, FRIESEN A, IBING L, KLEIN S, WINTER M, NOWAK S. Possible carbon-carbon bond formation during decomposition? Characterization and identification of new decomposition products in lithium ion battery electrolytes by means of SPME-GC-MS[J]. Electrochimica Acta, 2019, 295: 401 - 409 . doi: 10.1016/j.electacta.2018.08.159

[23]

SIM R, LANGDON J, MANTHIRAM A. Design of an online electrochemical mass spectrometry system to study gas evolution from cells with lean and volatile electrolytes[J]. Small Methods, 2023, 7(6): e2201438. doi: 10.1002/smtd.202201438

[24]

FANG C, TRAN T N, ZHAO Y, LIU G. Electrolyte decomposition and solid electrolyte interphase revealed by mass spectrometry[J]. Electrochimica Acta, 2021, 399: 139 362.

[25]

KOSTERS K, HENSCHEL J, WINTER M, NOWAK S. Online sample pretreatment for analysis of decomposition products in lithium ion battery by liquid chromatography hyphenated with ion trap-time of flight-mass spectrometry or inductively coupled plasma-sector field-mass spectrometry[J]. Journal of Chromatography A, 2021, 1 658: 462 594.

[26]

HENSCHEL J, PESCHEL C, KLEIN S, HORSTHEMKE F, WINTER M, NOWAK S. Clarification of decomposition pathways in a state-of-the-art lithium ion battery electrolyte through ¹³C-labeling of electrolyte components[J]. Angewandte Chemie International Edition, 2020, 59(15): 6 128-6 137.

[27]

PESCHEL C, HORSTHEMKE F, LEIßING M, WIEMERS-MEYER S, HENSCHEL J, WINTER M, NOWAK S. Analysis of carbonate decomposition during solid electrolyte interphase formation in isotope-labeled lithium ion battery electrolytes: extending the knowledge about electrolyte soluble species[J]. Batteries & Supercaps, 2020, 3(11): 1 183-1 192.

[28]

FANG C, LAU J, HUBBLE D, KHOMEIN P, DAILING E A, LIU Y, LIU G. Large-molecule decomposition products of electrolytes and additives revealed by on-electrode chromatography and MALDI[J]. Joule, 2021, 5(2): 415 - 428 . doi: 10.1016/j.joule.2020.12.012

[29]

WILKEN S, TRESKOW M, SCHEERS J, JOHANSSON P, JACOBSSON P. Initial stages of thermal decomposition of LiPF₆-based lithium ion battery electrolytes by detailed Raman and NMR spectroscopy[J]. RSC Advances, 2013, 3(37): 16 359.

[30]

LIAO Z, ZHANG J, GAN Z, WANG Y, ZHAO J, CHEN T, ZHANG G. Thermal runaway warning of lithium-ion batteries based on photoacoustic spectroscopy gas sensing technology[J]. International Journal of Energy Research, 2022, 46(15): 21 694-21 702.

[31]

LARSSON F, BERTILSSON S, FURLANI M, ALBINSSON I, MELLANDER B E. Gas explosions and thermal runaways during external heating abuse of commercial lithium-ion graphite-LiCoO₂ cells at different levels of ageing[J]. Journal of Power Sources, 2018, 373: 220 - 231 . doi: 10.1016/j.jpowsour.2017.10.085

[32]

HILDEBRAND S, FERRARIO F, LEBEDEVA N. Comparative overview of methods for the detection of airborne electrolyte components released from lithium-ion batteries[J]. Energy Technology, 2023, 12(1): 2 300 647.

[33]

金淑聪, 吕警, 王景. 便携式吹扫捕集-GC/MS现场快速监测水中苯系物[J]. 生物化工, 2021, 7(3): 22 - 25 . doi: 10.3969/j.issn.2096-0387.2021.03.006 JIN Shucong, LYU Jing, WAN Jing. Portable purge and trap-GC/MS on-site rapid monitoring of benzene series[J]. Biological Chemical Engineering, 2021, 7(3): 22 - 25 (in Chinese). doi: 10.3969/j.issn.2096-0387.2021.03.006

[34]

QIU J, XU K, ZHANG T, ZHU H, ZHANG S, LU X, LI X. Development of a portable gas chromatography linear ion trap mass spectrometer (GC-LIT-MS) for VOCs analysis in water[J]. International Journal of Mass Spectrometry, 2024, 497: 117 189.

[35]

MASASHI Y, KATSUMI T. New method for determining antoine constants[J]. Journal of Chemical Engineering of Japan, 2010, 43(9): 727 - 729 . doi: 10.1252/jcej.10we047

[36]

RAHIMI P, WARD C. Kinetics of evaporation: statistical rate theory approach[J]. International Journal of Thermodynamics, 2010, 8(1): 1 - 14 .

[37]

BARRETT J, CLEMENT C. Kinetic evaporation and condensation rates and their coefficients[J]. Journal of Colloid and lnterface Science, 1992, 150(2): 352 - 364 . doi: 10.1016/0021-9797(92)90205-Z

[38]

李守信, 陈青松, 罗鑫, 张文, 曾华英. 吸附法处理VOCs脱附温度的选择[J]. 中国环保产业, 2018(3): 48 - 50 . doi: 10.3969/j.issn.1006-5377.2018.03.012 LI Shouxin, CHEN Qingsong, LUO Xin, ZHANG Wenzhi, ZENG Huaying. Determination on desorbing temperature of VOCs treated by adsorption method[J]. China Environmental Protection Industry, 2018(3): 48 - 50 (in Chinese). doi: 10.3969/j.issn.1006-5377.2018.03.012

[39]

SUN X, FAN X, HUANG W, DONG L, SUN Y. Influence of pressure and temperature on the toluene desorption from activated carbon under supercritical CO₂[J]. Case Studies in Thermal Engineering, 2023, 52: 103 677.

[40]

THOMPSON L M, STONE W, ELDESOKY A, SMITH N K, MCFARLANE C R M, KIM J S, JOHNSON M B, PETIBON R, DAHN J R. Quantifying changes to the electrolyte and negative electrode in aged NMC532/graphite lithium-ion cells[J]. Journal of the Electrochemical Society, 2018, 165(11): A2732-A2740.