内部萃取电喷雾电离质谱法快速测定不同产地酸枣仁中脂肪酸含量

刘鹏; 王宁; 谢斯瑜; 王乐婷; 梁哲豪; 赖润晨; 秦嫚嫚

doi:10.7538/zpxb.2024.0173

[1]

WANG D, HO C T, BAI N. Ziziphi Spinosae Semen: an updated review on pharmacological activity, quality control, and application[J]. Journal of Food Biochemistry, 2022, 46(7): e14153.

[2]

ZHU C, ZHANG Z, WANG S, SUN Z. Study on the mechanism of Gastrodiae Rhizoma, Lycii Fructus, and Ziziphi Spinosae Semen in sedation and tranquillising mind[J]. Molecular Diversity, 2024, 28(5): 3 279-3 294.

[3]

XIE J, GUO L, PANG G, WU X, ZHANG M. Modulation effect of Semen Ziziphi Spinosae extracts on IL-1β, IL-4, IL-6, IL-10, TNF-α and IFN-γ in mouse serum[J]. Natural Product Research, 2011, 25(4): 464 - 467 .

[4]

ZHANG M, LIU J, ZHANG Y, XIE J. Ziziphi Spinosae Semen: a natural herb resource for treating neurological disorders[J]. Current Topics in Medicinal Chemistry, 2022, 22(17): 1 379-1 391.

[5]

刘薇, 李明华, 余坤子, 程显隆, 魏锋, 马双成. 中药酸枣仁的真伪鉴别方法研究[J]. 药物分析杂志, 2015, 35(9): 1 629-1 634. LIU Wei, LI Minghua, YU Kunzi, CHENG Xianlong, WEI Feng, MA Shuangcheng. Quality analysis of Ziziphi Spinosae Semen and identification of adulterants[J]. Chinese Journal of Pharmaceutical Analysis, 2015, 35(9): 1 629-1 634(in Chinese).

[6]

DU C, HAN R, WU J, ZHAO N, PEI X, QIN X, YAN Y. Study on the antidepressive effects and mechanism of raw and fried Ziziphi Spinosae Semen via metabolomics and gut microbiota analysis[J]. Biomedical Chromatography, 2024, 38(7): e5873.

[7]

XIE J, ZHANG Y, WANG L, QI W, ZHANG M. Composition of fatty oils from Semen Ziziphi Spinosae and its cardiotonic effect on isolated toad hearts[J]. Natural Product Research, 2012, 26(5): 479 - 483 .

[8]

ABDO A, ZHANG C, AL-DALALI S, HOU Y, GAO J, YAHYA M A, SALEH A, ALERYANI H, AL-ZAMANI Z, SANG Y. Marine chitosan-oligosaccharide ameliorated plasma cholesterol in hypercholesterolemic hamsters by modifying the gut microflora, bile acids, and short-chain fatty acids[J]. Nutrients, 2023, 15(13): 2 923.

[9]

SIMARD M, TREMBLAY A, MORIN S, MARTIN C, JULIEN P, FRADETTE J, FLAMAND N, POULIOT R. α-Linolenic acid and linoleic acid modulate the lipidome and the skin barrier of a tissue-engineered skin model[J]. Acta Biomaterialia, 2022, 140: 261 - 274 .

[10]

ZHAO X, YU D, ZHOU W, YU L, ZHOU H, LIU Y, GUO Z, SHEN A, HAN Z, WANG C, WANG J, LIANG X. Chemical profiling of Ziziphi Spinosae Semen using on-line comprehensive two-dimensional liquid chromatography-mass spectrometry based on a novel phthalic anhydride bonded stationary phase[J]. Journal of Separation Science, 2023, 46(10): 2 200 704.

[11]

MORADI S, ALIVAND M, KHAJEBISHAK Y, ASGHARIJAFARABADI M, ALIPOUR M, CHILIBECK P D, ALIPOUR B. The effect of omega3 fatty acid supplementation on PPARγ and UCP2 expressions, resting energy expenditure, and appetite in athletes[J]. BMC Sports Science, Medicine & Rehabilitation, 2021, 13(1): 48.

[12]

IMIG J D. Bioactive lipids in hypertension[J]. Advances in Pharmacology, 2023, 97: 1 - 35 .

[13]

MORANO C, DEI CAS M, BERGAMASCHI R F, PALMISANO E, PALLAVICINI M, BOLCHI C, RODA G, CASATI S. Fractioning and compared 1H NMR and GC-MS analyses of lanolin acid components[J]. Molecules, 2023, 28(4): 1 635.

[14]

LI Y J, BI K S, LIANG X M, XIAO H B. Analysis of fatty oil in Semen Ziziphi Spinosae by capillary gas chromatography[J]. Journal of Chromatographic Science, 2003, 41(1): 41 - 43 .

[15]

YOUNIS I Y, KHATTAB A R, SELIM N M, SOBEH M, ELHAWARY S S, BISHBISHY M H E. Metabolomics-based profiling of 4 avocado varieties using HPLC-MS/MS and GC/MS and evaluation of their antidiabetic activity[J]. Scientific Reports, 2022, 12(1): 4 966.

[16]

GARCÍA MARTÍN J F. Potential of near-infrared spectroscopy for the determination of olive oil quality[J]. Sensors, 2022, 22(8): 2 831.

[17]

QIAN J, ZHAO C, ZHU H, TONG J, ZHAO X, YANG H, GUO H. NMR detection of fatty acidscontent in walnut oil and compared with liquid chromatography[J]. Journal of Food Measurement and Characterization, 2021, 15(3): 2 716-2 726.

[18]

BAVISKAR K P, JAIN D V, PINGALE S D, WAGH S S, GANGURDE S P, SHARDUL S A, DAHALE A R, JAIN K S. A review on hyphenated techniques in analytical chemistry[J]. Current Analytical Chemistry, 2022, 18(9): 956 - 976 .

[19]

陈焕文. 内部萃取电喷雾电离质谱研究进展[C]//2018年中国质谱学术大会(CMSC 2018)论文集. 广州, 2018: 225.

[20]

QIN M, QIAN Y, HUANG L, ZHONG C, LI M, YU J, CHEN H. Extractive electrospray ionization mass spectrometry for analytical evaluation and synthetic preparation of pharmaceutical chemicals[J]. Frontiers in Pharmacology, 2023, 14: 1 110 900.

[21]

ZHANG H, CHINGIN K, LI J, LU H, HUANG K, CHEN H. Selective enrichment of phosphopeptides and phospholipids from biological matrixes on TiO₂ nanowire arrays for direct molecular characterization by internal extractive electrospray ionization mass spectrometry[J]. Analytical Chemistry, 2018, 90(20): 12 101-12 107.

[22]

XIAO Y P, LU H Y, LÜ S J, XIE S X, WANG Z Z, CHEN H W. Rapid analysis of trace salbutamol and clenbuterol in pork samples by mass spectrometry[J]. Chinese Journal of Analytical Chemistry, 2016, 44(11): 1 633-1 638.

[23]

KOU W, ZHANG H, BIBI A, KE M, HAN J, XIONG J, SU R, LIANG D. Fast quantification of fluoroquinolones in environmental water samples using molecularly imprinted polymers coupled with internal extractive electrospray ionization mass spectrometry[J]. RSC Advances, 2018, 8(31): 17 293-17 299.

[24]

TAMURA P, FRUEHAN C, JOHNSON D K, HINKES P, WILLIAMS T D, WELTI R. Fatty acid composition by total acyl lipid collision-induced dissociation time-of-flight (TAL-CID-TOF) mass spectrometry[M]//Plant Lipids. New York, NY: Springer US, 2021: 117-133.

[25]

DING J, GU H, YANG S, LI M, LI J, CHEN H. Selective detection of diethylene glycol in toothpaste products using neutral desorption reactive extractive electrospray ionization tandem mass spectrometry[J]. Analytical Chemistry, 2009, 81(20): 8 632-8 638.

[26]

SHRIVASTAVA A, GUPTA V. Methods for the determination of limit of detection and limit of quantitation of the analytical methods[J]. Chronicles of Young Scientists, 2011, 2(1): 21 .

[27]

ZHAO J, LI S P, YANG F Q, LI P, WANG Y T. Simultaneous determination of saponins and fattyacids in Ziziphus jujuba (Suanzaoren) by high performance liquid chromatography-evaporative light scattering detection and pressurized liquid extraction[J]. Journal of Chromatography A, 2006, 1 108(2): 188-194.

[28]

琚思伟. 陕北黄河沿岸酸枣种源研究[D]. 杨凌: 西北农林科技大学, 2023.