磁质谱高丰度灵敏度阻滞过滤器研制与性能测试

袁祥龙; 沈小攀; 翟利华; 李飞腾; 邓虎; 徐江; 冯磊; 李志明

doi:10.7538/zpxb.2024.1008

[1]

赵墨田. 低丰度同位素质谱分析法[J]. 质谱学报, 1994, 15(1): 8 - 15 . ZHAO Motian. A method for the mass spectrometric measurement of low abundance isotopes[J]. Journal of Chinese Mass Spectrometry Society, 1994, 15(1): 8 - 15 (in Chinese).

[2]

HABFAST K, LAUE H J. Magnetic sector mass spectrometer with very high abundance sensitivity[C]. Proceedings of the Alfred O Nier Symposium on Inorganic Mass Spectrometry, 1991, Durango, CO, Los Alamos Report LA-12522, 1993: 75-91.

[3]

FREEMAN N J, DALY N R, POWELL R E. Retardation lens used to improve the abundance sensitivity of a mass spectrometer[J]. Review of Scientific Instruments, 1967, 38(7): 945 - 948 . doi: 10.1063/1.1720931

[4]

SMITH D H, CHRISTIE W H, McKOWN H S, WALKER S L, HERTEL G R. A new three-stage mass spectrometer for high abundance sensitivity measurements[J]. International Journal of Mass Spectrometry and Ion Physics, 1973, 10(3): 343 - 351 . doi: 10.1016/0020-7381(73)83011-6

[5]

STOFFELS J J, ELLS D R, BOND L A, FREEDMAN P A, TATTERSALL B N, LANGERGREN C R. A triple-sector mass spectrometer with high transmission efficiency and 10-11 isotope-abundance sensitivity[J]. International Journal of Mass Spectrometry and Ion Processes, 1994, 132(3): 217 - 224 . doi: 10.1016/0168-1176(93)03943-G

[6]

ZHANG Z B. A high abundance sensitivity mass spectrometer with double-directaional focus[J]. Nuclear Instruments and Methods in Physics Research, 1987, B26: 377 - 380 .

[7]

PALACZ Z A, FREEDMAN P A, WALDER A J. Thorium isotope ratio measurements at high abundance sensitivity using a VG54-30^®, an energy-filtered thermal ionization mass spectrometer[J]. Chemical Geology: Isotope Geoscience Section, 1992, 101(1/2): 157 - 165 .

[8]

LUO X, REHKÄMPER M, LEE D C, HALLIDAY A N. High precision ²³⁰Th/²³²Th and ²³⁴U/²³⁸U measurements using energyfiltered ICP magnetic sector multiple collector mass spectrometry[J]. International Journal of Mass Spectrometry and Ion Processes, 1997, 171(1/2/3): 105 - 117 .

[9]

WALDER A J, FREEDMAN P A. Communication. Isotopic ratio measurement using a double focusing magnetic sector mass analyser with an inductively coupled plasma as an ion source[J]. Journal of Analytical Atomic Spectrometry, 1992, 7(3): 571 . doi: 10.1039/ja9920700571

[10]

韦冠一, 李志明, 翟利华, 徐江, 沈小攀, 张子斌. 磁-电-四极杆级联质谱中的离子光学设计[J]. 质谱学报, 2014, 35(3): 238 - 243 . WEI Guanyi, LI Zhiming, ZHAI Lihua, XU Jiang, SHEN Xiaopan, ZHANG Zibin. Ion optics design in magnet-electric-quadrupole tandem mass spectrometer[J]. Journal of Chinese Mass Spectrometry Society, 2014, 35(3): 238 - 243 (in Chinese).

[11]

WEI G, ZHAI L, LI Z, DENG H, XU J, ZHOU G, ZHANG Z. A novel magnetic-electric-quadrupole tandem mass spectrometer of ultra-high abundance sensitivity[J]. International Journal of Mass Spectrometry, 2013(343/344): 9 - 14 .

[12]

FREEMAN N J, DALY N R. An improved abundance sensitivity for a tandem mass spectrometer by means of a retardation lens[J]. Journal of Scientific Instruments, 1967, 44(11): 956 - 958 . doi: 10.1088/0950-7671/44/11/419

[13]

KAISER K, STEVENS C. Ion-retarding lens to improve the abundance sensitivity of tandem mass spectrometers[C]. ANL-7393, Engineering and Equipment (TID-4500), AEC Research and Development Report, Argonne National Laboratory, 1967: 1-10.

[14]

IRELAND T R, CLEMENT S, COMPSTON W, FOSTER J J, HOLDEN P, JENKINS B, LANC P, SCHRAM N, WILLIAMS I S. Development of shrimp[J]. Australian Journal of Earth Sciences, 2008, 55(6/7): 937 - 954 .

[15]

吕洪猷, 肖美琴. 提高质谱计灵敏度的离子减速透镜[J]. 质谱学报, 1994, 16(2): 74 - 76 . LYU Hongyou, XIAO Meiqin. Ion-retarding lens to improve the abundance sensitivity of mass spectrometer[J]. Journal of Chinese mass spectrometry Society, 1994, 16(2): 74 - 76 (in Chinese).

[16]

van CALSTEREN P, SCHWIETERS J B. Performance of a thermal ionisation mass spectrometer with a deceleration lens system and post-deceleration detector selection[J]. International Journal of Mass Spectrometry and Ion Processes, 1995(146/147): 119 - 129 . doi: 10.1016/0168-1176(95)04208-3

[17]

张舸, 邓辉, 张春华. RPQ-IC检测系统测量低丰度铀同位素[J]. 质谱学报, 2004, 25(3): 160 - 162 . ZHANG Ge, DENG Hui, ZHANG Chunhua. Determination of low abundance uranium isotope by RPQ-IC collector system[J]. Journal of Chinese Mass Spectrometry Society, 2004, 25(3): 160 - 162 (in Chinese).

[18]

WIESER M E, SCHWIETERS J B. The development of multiple collector mass spectrometry for isotope ratio measurements[J]. International Journal of Mass Spectrometry, 2005, 242(2/3): 97 - 115 .

[19]

SCOTT S R, SIMS K W W, REAGAN M K, BALL L, SCHWIETERS J B, BOUMAN C, LLOYD N S, WATERS C L, STANDISH J J, TOLLSTRUP D L. The application of abundance sensitivity filters to the precise and accurate measurement of uranium series nuclides by plasma mass spectrometry[J]. International Journal of Mass Spectrometry, 2019, 435: 321 - 332 . doi: 10.1016/j.ijms.2018.11.011

[20]

EILER J M, CLOG M, MAGYAR P, PIASECKI A, SESSIONS A, STOLPER D, DEERBERG M, SCHLUETER H J, SCHWIETERS J. A high-resolution gas-source isotope ratio mass spectrometer[J]. International Journal of Mass Spectrometry, 2013, 335: 45 - 56 . doi: 10.1016/j.ijms.2012.10.014

[21]

BOULYGA S F, KLÖTZLI U, PROHASKA T. Improved abundance sensitivity in MC-ICP-MS for determination of ²³⁶U/²³⁸U isotope ratios in the 10⁻⁷ to 10⁻⁸ range[J]. Journal of Analytical Atomic Spectrometry, 2006, 21(12): 1 427-1 430.

[22]

ANDERSEN M B, STIRLING C H, POTTER E K, HALLIDAY A N. Toward epsilon levels of measurement precision on ²³⁴U/²³⁸U by using MC-ICP MS[J]. International Journal of Mass Spectrometry, 2004, 237(2/3): 107 - 118 .

[23]

SAHOO S K, NAKAMURA Y, SHIRAISHI K, MASUDA A. Accurate measurement of uranium isotope ratios in soil samples using thermal ionization mass spectrometry equipped with a warp energy filter[J]. International Journal of Environmental Analytical Chemistry, 2004, 84(12): 919 - 926 . doi: 10.1080/03067310410001729015

[24]

黄淑清, 聂宜如, 申先甲. 热学教程[M]. 北京: 高等教育出版社, 1994: 257-261.

[25]

王欲知, 陈旭. 真空技术[M]. 北京: 北京航空航天大学出版社, 2007: 249-251.

[26]

CHEN Y, ZHAI L, DENG H, YUAN X, LI Z, ZHANG Q. The design of electrostatic quadrupole zoom lens for fixed multi-collector system at mass spectrometer[J]. International Journal of Mass Spectrometry, 2016, 408: 1 - 8 . doi: 10.1016/j.ijms.2016.09.001

[27]

YUAN X, LI Z, ZHAI L, XU J, SHEN X, DENG H, WANG W. Improvement of electrostatic quadrupole zoom lens for fixed multi-collector system in LRI-MS[C]. International Mass Spectrometry Conference, Florence (Italy), 2018: 359-361.