用APCI/ESI LC/MS跟踪烷基二苯醚磺化反应

金燕

doi:10.3969/j.issn.1004-2997.2001.01.003

质谱学报

用APCI/ESI LC/MS跟踪烷基二苯醚磺化反应

金燕. 2001: 用APCI/ESI LC/MS跟踪烷基二苯醚磺化反应, 质谱学报, 22(1): 15-20. doi: 10.3969/j.issn.1004-2997.2001.01.003

引用本文:

金燕. 2001: 用APCI/ESI LC/MS跟踪烷基二苯醚磺化反应, 质谱学报, 22(1): 15-20. doi: 10.3969/j.issn.1004-2997.2001.01.003

Jin Yan. 2001: racing Analysis of Sulfonation of Alkyl Diphenyl Ether by APCI/ESI HPLC/MS, Journal of Chinese Mass Spectrometry Society, 22(1): 15-20. doi: 10.3969/j.issn.1004-2997.2001.01.003

Citation:

Jin Yan. 2001: racing Analysis of Sulfonation of Alkyl Diphenyl Ether by APCI/ESI HPLC/MS, Journal of Chinese Mass Spectrometry Society, 22(1): 15-20. doi: 10.3969/j.issn.1004-2997.2001.01.003

用APCI/ESI LC/MS跟踪烷基二苯醚磺化反应

金燕

上海白猫有限公司研究所

通讯作者: 金燕

racing Analysis of Sulfonation of Alkyl Diphenyl Ether by APCI/ESI HPLC/MS

Jin Yan

Corresponding author: Jin Yan

摘要: 采用APCI/ESI LC-MS对烷基二苯醚磺化反应过程进行跟踪分析，通过高压液相色谱及大气压质谱对产物分离并鉴定，从而对产物结构进行定性。
- 烷基二苯醚烷基二苯醚磺酸盐高效液相色谱 /
- APCI/ESI质谱
Abstract: Tracing analysis was applied in the process of sulfonation of alkyl diphenyl ether by APCI/ ESI HPI S/MS. The sulfonated products were separated by HPLC and then detected by on- line MS. In this way, the components and structures were determined and charactered.